.: Experimental procedures

Hydrothermal and related methods
High pressure reactor Berghof – BR100 http://www.berghof.com/en/products/laboratory-equipment/reactors/high-pressure-reactors/br-100/	Microwave system Berghof – Speedwave 2 http://www.berghof.com/en/products/laboratory-equipment/digestion-technology/microwave-digestion/speedwave-2/

Structure and microstructure characterization techniques

“Ilie Murgulescu” Institute of Physical Chemistry Infrastructure by IFRANANOCHEM project - http://www.icf.ro/

· X- ray diffraction (XRD);

· Raman spectroscopy;

· Scanning electron microscopy (SEM);

· Transmission electron microscopy (TEM);

· X-ray photoelectron spectroscopy (XPS);

· Thermogravimetric analysis (TGA) and Differential scanning calorimetry (DSC);

· Brunauer–Emmett–Teller (BET) measurements; etc.

Electrical and Thermodynamic characterization
Impedance Spectroscopy – HF FRA Solartron SI 1255 http://www.solartronanalytical.com/our-products/fra/Model-1255b-frequency-response-analyzer.aspx	Electromotive force measurements  http://www.icf.ro/L2.htm

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